Nucleation Control for Large, Single Crystalline Domains of Mono layer Hexagonal Boron Nitride via Si-Doped Fe Catalysts

Author(s)
Sabina Caneva, Robert S. Weatherup, Bernhard C. Bayer, Barry Brennan, Steve J. Spencer, Ken Mingard, Andrea Cabrero-Vilatela, Carsten Baehtz, Andrew J. Pollard, Stephan Hofmann
Abstract

The scalable chemical vapor deposition of monolayer hexagonal boron nitride (h-BN) single crystals, with lateral dimensions of similar to 0.3 mm, and of continuous h-BN monolayer films With large domain sizes (>25 mu m) is demonstrated via an admixture of Si to Fe catalyst films. A simple thin-filth Fe/'SiO2/Si catalyst system is used to show that controlled Si diffusion into the Fe catalyst allows exclusive nucleation of monolayer h-BN with very low nucleation densities upon exposure to undiluted borazine. Our systematic in situ and ex situ characterization of this catalyst system establishes, a basis for further rational catalyst design for compound 2D materials.

Organisation(s)
Physics of Nanostructured Materials
External organisation(s)
University of Cambridge, Helmholtz-Zentrum Dresden-Rossendorf, National Physical Laboratory
Journal
Nano Letters: a journal dedicated to nanoscience and nanotechnology
Volume
15
Pages
1867-1875
No. of pages
9
ISSN
1530-6984
DOI
https://doi.org/10.1021/nl5046632
Publication date
03-2015
Peer reviewed
Yes
Austrian Fields of Science 2012
210006 Nanotechnology, 103018 Materials physics
Keywords
ASJC Scopus subject areas
Condensed Matter Physics, Mechanical Engineering, Bioengineering, Chemistry(all), Materials Science(all)
Portal url
https://ucrisportal.univie.ac.at/en/publications/nucleation-control-for-large-single-crystalline-domains-of-mono-layer-hexagonal-boron-nitride-via-sidoped-fe-catalysts(7617d54c-98f0-42cd-975d-c728b24814d8).html