The formation of supersaturated solid solutions in Fe-Cu alloys deformed by high-pressure torsion

Author(s)
Andrea Bachmaier, Michael Kerber, Daria Setman, Reinhard Pippan
Abstract

Fully dense bulk nanocomposites have been obtained by a novel two-step severe plastic deformation process in the immiscible Fe-Cu system. Elemental micrometer-sized Cu and Fe powders were first mixed in different compositions and subsequently high-pressure-torsion-consolidated and deformed in a two-step deformation process. Scanning electron microscopy, X-ray diffraction and atom probe investigations were performed to study the evolving far-from-equilibrium nanostructures which were observed at all compositions. For lower and higher Cu contents complete solid solutions of Cu in Fe and Fe in Cu, respectively, are obtained. In the near 50% regime a solid solution face-centred cubic and solid solution body-centred cubic nanograined composite has been formed. After an annealing treatment, these solid solutions decompose and form two-phase nanostructured Fe-Cu composites with a high hardness and an enhanced thermal stability. The grain size of the composites retained nanocrystalline up to high annealing temperatures.

Organisation(s)
Physics of Nanostructured Materials
External organisation(s)
Österreichische Akademie der Wissenschaften (ÖAW)
Journal
Acta Materialia
Volume
60
Pages
860-871
No. of pages
12
ISSN
1359-6454
DOI
https://doi.org/10.1016/j.actamat.2011.10.044
Publication date
2012
Peer reviewed
Yes
Austrian Fields of Science 2012
210006 Nanotechnology, 103018 Materials physics
Portal url
https://ucrisportal.univie.ac.at/en/publications/748acf22-ecea-4e74-a8c3-ce7b608f28d5